The FRX300 system is supplied with 3 pumps enabling up to three inputs into a reactions or two inputs and an immiscible aqueous work-up stream.
The FLLEX module combines two immiscible phases in a mixer to give rapid partitioning, then separates the two phases as a continual flow process. Due to the nature of the mixing, emulsions are reduced and because of the superior method of separation, solvent pairs that would not normally be used in batch work-ups are possible in the FLLEX e.g. THF/aqueous and toluene/aqueous.
Reaction optimisation and preparative synthesis are possible using a range of different reactors (a microrector, tube reactor and 4 solid-phase columns). The inclusion of solid phase columns allows solid supported reagents, scavengers and catalysts to be used.
The system also includes a Pressurisation Module, enabling operation above solvent boiling points, and a Collection Module which allows manual collection of different fractions of products as reaction conditions change.
All of the tubing required to connect the modules is provided cut to length, terminated with connectors and labelled for convenience. Extra tubing and connectors are also supplied in the form of a Flow Tubing Starter Pack. A Pneumatic Adaptor Pack is included in the FRX300 system to allow easy connection of the Pressurisation Module to a variety of common laboratory gas fittings.
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The FRX300 System contains the following modules:
Description Part Number
3 FRX Pumps - 2101305
FRX Reagent Module (Including 2 x 5ml Sample Loops) - 2101308
FRX Volcano (With 1 x Microreactor and 2 x Column Adaptors) - 2101311
250µl Microreactor Chip 2 Input - 2100143
4ml Tube Reactor PTFE - 2100632
FRX Column Pack (1 of Each Size) - 2101345
FRX IKA Hotplate - 2101310
FRX Pressurisation Module 2101307
FRX FLLEX Module - 2101306
FRX Collection Module - 2101309
Chip Header - 2100147
Tube Reactor 3 Input Adaptor (PCTFE) - 2100915
Tube Reactor Ring Set - 2100838
FRX Collection Needle - 2101381
FRX Pneumatic Adaptor Pack - 2101352
Flow Tubing Starter Pack - 2110713
FRX 300 Plumbing Set - 2101402